Dehydration of 2-Methylclyclohexanol, Tests for Unsaturation, and Gas Chromatography

Ashley Peccatiello Experiment 7 Dehydration of 2-Methylclyclohexanol, Tests for Unsaturation, and Gas Chromatography go pissed Performed: October 25, 2012 Date Written: October 29, 2012 Purpose: To dehydrate 2-methylclyclohexanol to obtain devil isomers. To carve up the mathematical products by simple distillation. To try out the archetype by introducing the technique of gas chromatography and unsaturation tests. Reaction: range 1. Overall reaction of the acrimonious-catalyzed dehydration of 2-methylcyclohexanol Figure 2. Reactions for the unsaturation tests hold over of Reactants and Products: Table 1. Molecular weight, density, melting point, and boiling point for all reagents utilize in Experiment #7 Dehydration of 2-Methylclyclohexanol, Tests for Unsaturation, and Gas Chromatography. find:| MW (g/mol):| Density (g/mL):| MP (C):| BP (C):| MSDS:| 2-methylcyclohexanol| 114.19| 0.93| -38.00| 165-168| Irritant, combustible| 95% phospho ric acid| 97.994| 1.69| 42.35| 158| Corrosive, irritant| 1-methylcyclohexene| 96.17| 0.81| -120.4| 110| Irritant, flammable| 3-methylcyclohexene| 96.17| 0.81| -124.

00| 104| Irritant, flammable| Procedure: luck One Dehydration of 2-methylcyclohexanol A microdistillation apparatus was assembled by secu banding a microdistillation flaskful to a ring stand and submerging it in an empty heating mantle. A thermometer and Teflon adaptor were tightly sealed into the top of the flask with the thermometer myeline beingness below the side arm. The collection flask was secured at the fetch up of the side arm. Sand was added to the heating cape until the fl! ask bulb was mostly covered. The heating mantel was machine-accessible to a variac anterior to the outlet. A boiling stone, 1 mL of 2-methylcyclohexanol, and 2 mL of 85% phosphoric acid was added to the flask. The sample was heated gently, retention the temperature below 96C, until .5 mL of distillate was collected. The product was dried utilize calcium chloride for approximately 10 minutes....If you necessitate to get a full essay, order it on our website: BestEssayCheap.com

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